Clowder
  1. ReGen
  2. Gen 0

Gen 0

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Description:

ReGen experiment uploaded by remat-data CLI

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Metadata

Name Value Last Modified
DSC Procedure
  • DSC Procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: AR-37_DCPD_1k__Gen1_liquid_CK_C
    • Sample Mass (mg): 3.000 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 7/9/2024 1:58:21 PM
    • Operator: AR
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.1.74
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 200.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 334.28
    • Peak temperature (°C): 71.13
    • Onset x (°C): 61.22
    • Max Heat Flow: 7.29
    • Min Baseline Temp: 25.707
    • Max Baseline Temp: 111.958
Extracted by https://re-mat.clowderframework.org/api/extractors/remat.parameters.from_txt on Jul 22, 2026
Batch ID
  • Batch ID: 09-7-2024 00:00 AR
  • procedure:
    • general:
      • Operator Initials: AR
      • Mix Date and Time: 2024-07-09T00:00:00
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 3
      • Preparation temperature (°C): 20
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: Printing
      • TRIAL (NEED TO FILL): null
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
    • thermal initiation:
      • Heat Source: SOLDERING IRON
      • Heat Source Name: null
      • Heater diameter (mm): null
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): null
      • Current (A): null
      • Heat source temperature (°C): null
      • Induction time (s): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 8.55
          • Measured volume (μL): null
          • Computed mass (g): 8.55
          • Molecular Weight (g/mol): 120.2
          • Moles: 7.11e-02
          • Monomer mol%: 95.43
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 0.45
          • Measured volume (μL): null
          • Computed mass (g): 0.45
          • Molecular Weight (g/mol): 132.2
          • Moles: 3.40e-03
          • Monomer mol%: 4.57
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: null
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 62.145
          • Computed mass (g): 0.062145000000000006
          • Molecular Weight (g/mol): 848.98
          • Moles: 7.32e-05
          • Monomer:Catalyst molar ratio: 1018.25
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 19.8
          • Density: 0.925
          • Computed mass (g): 0.018315
          • Molecular Weight (g/mol): 250.3
          • Moles: 7.32e-05
          • Inhibitor:Catalyst molar ratio: 1.0
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
          • name: iPrSi8
          • SMILES: CC(C)[Si]1(C(C)C)OC/C=C\CCO1
          • Measured mass (g): 1.13
          • Measured volume (μL): null
          • Computed mass (g): 1.13
          • Molecular Weight (g/mol): 214.38
          • Moles: 5.27e-03
          • Wt Percent of Additives: 11.09
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): 0.67
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: LINEAR
  • regen:
    • oligomers:
      • is_root: true
      • parents:
      • procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • decon:
      • reagents:
          • Name: Tetrebutylammonium Phosphate (TBAF)
          • SMILES: [F-].CCCC[N+](CCCC)(CCCC)CCCC
          • Measured volume (mL): 115
          • Supplier: null
          • Lot #: null
      • procedure:
        • Prepared in GloveBox?: NO
        • Atmosphere: null
        • Deconstruction temperature (°C): null
        • Stirr: NO
        • Vial size (mL): null
        • Deconstruction time (hrs): null
        • Total volume used for deconstruction (mL): null
    • postproc:
      • STEP 1:
        • Process: Precipitate
        • Temperature (C) : 20
        • AntiSol 1: Methanol
      • STEP 2:
        • Process: Filter
        • Temperature (C) : 20
      • STEP 3:
        • Process: Drying
        • Temperature (C) : 20
    • results:
Extracted by https://re-mat.clowderframework.org/api/extractors/remat.experiment.from_excel on Jul 22, 2026
  • DSC Procedure:
    • Experiment Type: Liquid_CureKinetics
    • Sample Name: AR-37_DCPD_1k__Gen1_liquid_CK_C
    • Sample Mass (mg): 3.000 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 7/9/2024 1:58:21 PM
    • Operator: AR
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.7.1.74
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 200.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 334.28
    • Peak temperature (°C): 71.13
    • Onset x (°C): 61.22
    • Max Heat Flow: 7.29
    • Min Baseline Temp: 25.707
    • Max Baseline Temp: 111.958
  • Batch ID: 09-7-2024 00:00 AR
  • procedure:
    • general:
      • Operator Initials: AR
      • Mix Date and Time: 2024-07-09T00:00:00
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): null
      • Resin Storage atmosphere: null
      • Resin Storage location: null
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 3
      • Preparation temperature (°C): 20
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: FROMP
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: Printing
      • TRIAL (NEED TO FILL): null
      • Empty-dim: null
      • Initiation: null
      • Initiation method: THERMAL
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
    • thermal initiation:
      • Heat Source: SOLDERING IRON
      • Heat Source Name: null
      • Heater diameter (mm): null
      • Submerged length (mm): null
      • Power (W): null
      • Voltage (V): null
      • Current (A): null
      • Heat source temperature (°C): null
      • Induction time (s): null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 8.55
          • Measured volume (μL): null
          • Computed mass (g): 8.55
          • Molecular Weight (g/mol): 120.2
          • Moles: 7.11e-02
          • Monomer mol%: 95.43
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 0.45
          • Measured volume (μL): null
          • Computed mass (g): 0.45
          • Molecular Weight (g/mol): 132.2
          • Moles: 3.40e-03
          • Monomer mol%: 4.57
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: null
        • Mixing time (mins): null
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 62.145
          • Computed mass (g): 0.062145000000000006
          • Molecular Weight (g/mol): 848.98
          • Moles: 7.32e-05
          • Monomer:Catalyst molar ratio: 1018.25
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
          • name: TBP
          • SMILES: CCCCOP(=O)(OCCCC)OCCCC
          • Measured volume (μL): 19.8
          • Density: 0.925
          • Computed mass (g): 0.018315
          • Molecular Weight (g/mol): 250.3
          • Moles: 7.32e-05
          • Inhibitor:Catalyst molar ratio: 1.0
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
          • name: iPrSi8
          • SMILES: CC(C)[Si]1(C(C)C)OC/C=C\CCO1
          • Measured mass (g): 1.13
          • Measured volume (μL): null
          • Computed mass (g): 1.13
          • Molecular Weight (g/mol): 214.38
          • Moles: 5.27e-03
          • Wt Percent of Additives: 11.09
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
  • FROMP Measurements:
    • Measured frontal velocity (mm/s): 0.67
    • Measured frontal velocity with light exposure (mm/s): null
    • Measured maximum temperature (°C): null
    • Type of front: LINEAR
  • regen:
    • oligomers:
      • is_root: true
      • parents:
      • procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • decon:
      • reagents:
          • Name: Tetrebutylammonium Phosphate (TBAF)
          • SMILES: [F-].CCCC[N+](CCCC)(CCCC)CCCC
          • Measured volume (mL): 115
          • Supplier: null
          • Lot #: null
      • procedure:
        • Prepared in GloveBox?: NO
        • Atmosphere: null
        • Deconstruction temperature (°C): null
        • Stirr: NO
        • Vial size (mL): null
        • Deconstruction time (hrs): null
        • Total volume used for deconstruction (mL): null
    • postproc:
      • STEP 1:
        • Process: Precipitate
        • Temperature (C) : 20
        • AntiSol 1: Methanol
      • STEP 2:
        • Process: Filter
        • Temperature (C) : 20
      • STEP 3:
        • Process: Drying
        • Temperature (C) : 20
    • results:
Extractor Started Latest Update Latest Status
Submission Status
Timestamp Status Message
Wed Jul 22 20:52:39 UTC 2026 PROCESS: Uploading dataset metadata.
Submission Status
Timestamp Status Message
Wed Jul 22 20:52:37 UTC 2026 PROCESS: Uploading dataset metadata.

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Last viewed: Sep 15, 2026 13:42:56
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Last Modified: Jul 22, 2026 20:52:37

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