Clowder
  1. DSC Cure Kinetics
  2. 95/5 DCPD/ENB, ...

95/5 DCPD/ENB, 10 mol% DHF, 0.5 mol % BHT, 6 hr incubation, paired with 0 hr incubation - 1 of 3

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Description:

Incubated in shell vials under N2 at 25C for 6 hours. Placed into DSC at 5:38 PM on 7/16/2026. Part of Incubation-Topology Set Paired with 0 hr incubation

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Metadata

Name Value Last Modified
DSC Procedure
  • DSC Procedure:
    • Experiment Type: Liquid_CureKinetics_-20to180
    • Sample Name: 10molDHF_ML_07162026_6h-1
    • Sample Mass (mg): 4.460 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 7/16/2026 5:38:55 PM
    • Operator: ML
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.11.0.31
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 180.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 231.4
    • Peak temperature (°C): 70.9
    • Onset x (°C): 55.747
    • Max Heat Flow: 3.5
    • Min Baseline Temp: 25.0
    • Max Baseline Temp: 170.0
Extracted by https://re-mat.clowderframework.org/api/extractors/remat.parameters.from_txt on Aug 10, 2026
Batch ID
  • Batch ID: 16-7-2026 11:33 ML
  • procedure:
    • general:
      • Operator Initials: ML
      • Mix Date and Time: 2026-07-16T11:33:00
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): 25
      • Resin Storage atmosphere: N2
      • Resin Storage location: Oven
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 7
      • Preparation temperature (°C): 20
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: null
      • #N/A: null
      • Initiation: null
      • Initiation method: NONE
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.050315
          • Measured volume (μL): null
          • Computed mass (g): 0.050315
          • Molecular Weight (g/mol): 120.2
          • Moles: 4.19e-04
          • Monomer mol%: 4.95
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 0.955985
          • Measured volume (μL): null
          • Computed mass (g): 0.955985
          • Molecular Weight (g/mol): 132.2
          • Moles: 7.23e-03
          • Monomer mol%: 85.56
          • name: Dihydrofuran (DHF)
          • SMILES: C1COC=C1
          • Measured mass (g): 0.0562
          • Measured volume (μL): null
          • Computed mass (g): 0.0562
          • Molecular Weight (g/mol): 70.1
          • Moles: 8.02e-04
          • Monomer mol%: 9.49
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): 7
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 0.71
          • Computed mass (g): 0.0007099999999999999
          • Molecular Weight (g/mol): 848.98
          • Moles: 8.36e-07
          • Monomer:Catalyst molar ratio: 10106.04
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
          • name: Butylated hydroxytoluene (BHT)
          • SMILES: CC(C)(C)c1cc(C)cc(c1O)C(C)(C)C
          • Measured mass (g): 8.94
          • Measured volume (μL): null
          • Computed mass (g): 8.94
          • Molecular Weight (g/mol): 220.356
          • Moles: 4.06e-02
          • Wt Percent of Additives: 89.37
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): 7
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
Extracted by https://re-mat.clowderframework.org/api/extractors/remat.experiment.from_excel on Aug 10, 2026
  • DSC Procedure:
    • Experiment Type: Liquid_CureKinetics_-20to180
    • Sample Name: 10molDHF_ML_07162026_6h-1
    • Sample Mass (mg): 4.460 mg
    • Reference Pan Type: Tzero Aluminum Hermetic
    • Run Date: 7/16/2026 5:38:55 PM
    • Operator: ML
    • Instrument Name: DSC2A-01089
    • Instrument Type: DSC250
    • Serial Number: DSC2A-01089
    • Location of Instrument: Manufacturing Test
    • Trios version: 5.11.0.31
    • Ramp rate (°C/min): 7.0
    • Ramp Min Temp (°C): 5.0
    • Ramp Max Temp (°C): 180.0
  • Analysis:
    • Enthalpy (normalized)(J/g): 231.4
    • Peak temperature (°C): 70.9
    • Onset x (°C): 55.747
    • Max Heat Flow: 3.5
    • Min Baseline Temp: 25.0
    • Max Baseline Temp: 170.0
  • Batch ID: 16-7-2026 11:33 ML
  • procedure:
    • general:
      • Operator Initials: ML
      • Mix Date and Time: 2026-07-16T11:33:00
      • Polymerization Date and Time: null
      • Resin Storage Temperature (°C): 25
      • Resin Storage atmosphere: N2
      • Resin Storage location: Oven
      • Polymer Storage Temperature (°C): null
      • Polymer Storage armosphere: null
      • Polymer Storage location: null
      • Mixing Conditions: null
      • Mixing Type: Sonication
      • Mixing Time (min): 7
      • Preparation temperature (°C): 20
      • Use Glovebox: NO
      • Polymerization: null
      • Type of polymerization: NONE
      • Ambient temperature (°C): null
      • Resin temperaure at the start of polymerization (°C): null
      • Select Geometry from geometries tab: null
      • Geometry - Select from library: null
      • #N/A: null
      • Initiation: null
      • Initiation method: NONE
      • Photocontrol: null
      • Photocontrol?: NO
      • null: null
  • inputs:
    • monomers:
      • monomer-inputs:
          • name: Ethylidene Norbornene (ENB)
          • SMILES: CC=C1CC2CC1C=C2
          • Measured mass (g): 0.050315
          • Measured volume (μL): null
          • Computed mass (g): 0.050315
          • Molecular Weight (g/mol): 120.2
          • Moles: 4.19e-04
          • Monomer mol%: 4.95
          • name: Dicyclopentadiene (DCPD)
          • SMILES: C1C=CC2C1C3CC2C=C3
          • Measured mass (g): 0.955985
          • Measured volume (μL): null
          • Computed mass (g): 0.955985
          • Molecular Weight (g/mol): 132.2
          • Moles: 7.23e-03
          • Monomer mol%: 85.56
          • name: Dihydrofuran (DHF)
          • SMILES: C1COC=C1
          • Measured mass (g): 0.0562
          • Measured volume (μL): null
          • Computed mass (g): 0.0562
          • Molecular Weight (g/mol): 70.1
          • Moles: 8.02e-04
          • Monomer mol%: 9.49
      • monomer-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): 7
    • catalysts:
      • catalyst-inputs:
          • name: GC-2
          • SMILES: CC1=CC(=C(C(=C1)C)N2CCN(C2=[Ru](=CC3=CC=CC=C3)(Cl)Cl)C4=C(C=C(C=C4C)C)C)C.C1CCC(CC1)P(C2CCCCC2)C3CCCCC3
          • Measured mass (mg): 0.71
          • Computed mass (g): 0.0007099999999999999
          • Molecular Weight (g/mol): 848.98
          • Moles: 8.36e-07
          • Monomer:Catalyst molar ratio: 10106.04
      • catalyst-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): null
    • inhibitors:
      • inhibitor-inputs:
      • inhibitor-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
    • additives:
      • additive-inputs:
          • name: Butylated hydroxytoluene (BHT)
          • SMILES: CC(C)(C)c1cc(C)cc(c1O)C(C)(C)C
          • Measured mass (g): 8.94
          • Measured volume (μL): null
          • Computed mass (g): 8.94
          • Molecular Weight (g/mol): 220.356
          • Moles: 4.06e-02
          • Wt Percent of Additives: 89.37
      • additive-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: Sonication
        • Mixing time (mins): 7
    • solvents:
      • solvent-inputs:
      • solvent-procedure:
        • Prepared in GloveBox?: NO
        • Preparation temperature (°C): null
        • Mixing type: N/A
        • Mixing time (mins): null
Extractor Started Latest Update Latest Status
Submission Status
Timestamp Status Message
Mon Aug 10 22:23:30 UTC 2026 PROCESS: Uploading dataset metadata.
Submission Status
Timestamp Status Message
Mon Aug 10 22:23:29 UTC 2026 PROCESS: Uploading dataset metadata.

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Last viewed: Sep 15, 2026 12:46:30
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Last Modified: Aug 10, 2026 22:23:29

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